863408-46-2
- Product Name：2’OCEM-rA(Ac) phosphoramidite
- Molecular Formula：C46H55N8O9P
- Purity：99%
- Molecular Weight：894.965
Product Details;
CasNo： 863408-46-2
Molecular Formula： C46H55N8O9P
Factory Sells Best Quality 2’OCEM-rA(Ac) phosphoramidite 863408-46-2 with stock
- Molecular Formula:C46H55N8O9P
- Molecular Weight:894.965
863408-46-2 Relevant articles
A new RNA synthetic method with a 2′-O-(2-cyanoethoxymethyl) protecting group
Ohgi, Tadaaki,Masutomi, Yutaka,Ishiyama, Kouichi,Kitagawa, Hidetoshi,Shiba, Yoshinobu,Yano, Junichi
, p. 3477 - 3480 (2005)
(Chemical Equation Presented) A novel me...
METHOD FOR DETACHING PROTECTING GROUP ON NUCLEIC ACID
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Page/Page column 20, (2009/06/27)
A method is provided for removing a 2-cy...
METHOD FOR REMOVAL OF NUCLEIC ACID-PROTECTING GROUP
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Page/Page column 29, (2009/01/20)
The main object of the present invention...
PHOSPHORAMIDITE COMPOUND AND METHOD FOR PRODUCING OLIGO-RNA
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Page/Page column 26-27, (2010/11/27)
An object of the present invention is to...
863408-46-2 Process route
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863408-41-7
N6-acetyl-5′-O-(4,4′-dimethoxytrityl)-2′-O-(2-cyannethoxymethyl)adenosine
-
-
124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine
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863408-46-2
N6-acetyl-5'-O-(4,4'-dimethoxytrityl)-2'-O-(2-cyanoethoxymethyl)adenosine 3'-O-(2-cyanoethyl N,N-diisopropylphosphoramidite)
| Conditions | Yield |
|---|---|
|
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 1h;
|
93% |
|
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 1h;
|
93% |
|
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 1h;
|
93% |
|
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane;
at 20 ℃;
for 1h;
|
85% |
-
-
40615-36-9
4,4'-dimethoxytrityl chloride
-
-
863408-46-2
N6-acetyl-5'-O-(4,4'-dimethoxytrityl)-2'-O-(2-cyanoethoxymethyl)adenosine 3'-O-(2-cyanoethyl N,N-diisopropylphosphoramidite)
| Conditions | Yield |
|---|---|
|
Multi-step reaction with 3 steps
1: pyridine
2: 29 percent / N,N-diisopropylethylamine; dibutyltin dichloride / 1,2-dichloro-ethane / 1 h / 80 °C
3: 85 percent / N,N-diisopropylethylamine / CH2Cl2 / 1 h / 20 °C
With
pyridine; dibutyltin chloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; 1,2-dichloro-ethane;
|
863408-46-2 Upstream products
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863408-41-7
N6-acetyl-5′-O-(4,4′-dimethoxytrityl)-2′-O-(2-cyannethoxymethyl)adenosine
-
124482-92-4
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine
-
40615-36-9
4,4'-dimethoxytrityl chloride
-
231957-26-9
N6-acetyl-5'-O-(4,4'-dimethoxytrityl)adenosine
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