400607-04-7
- Product Name：Anthracene, 9-?bromo-?10-?(1-?naphthalenyl)?-
- Molecular Formula：C24H15Br
- Purity：99%
- Molecular Weight：383.287
Product Details;
CasNo： 400607-04-7
Molecular Formula： C24H15Br
Appearance： Yellow powder
Factory sells Anthracene, 9-?bromo-?10-?(1-?naphthalenyl)?- 400607-04-7 with sufficient production capacity
- Molecular Formula:C24H15Br
- Molecular Weight:383.287
- Appearance/Colour:Yellow powder
- Melting Point:177.0 to 181.0 °C
- Refractive Index:1.756
- Boiling Point:508 °C at 760 mmHg
- Flash Point:254.3 °C
- PSA：0.00000
- Density:1.403 g/cm3
- LogP:7.57570
Anthracene, 9-bromo-10-(1-naphthalenyl)-(Cas 400607-04-7) Usage
InChI:InChI=1/C24H15Br/c25-24-21-13-5-3-11-19(21)23(20-12-4-6-14-22(20)24)18-15-7-9-16-8-1-2-10-17(16)18/h1-15H
400607-04-7 Relevant articles
ANTHRACENE COMPOUND AND ORGANIC LIGHT EMITTING DEVICE COMPRISING SAME
-
Paragraph 0181-0183; 0194-0196, (2021/05/18)
The present specification relates to an ...
DOUBLE-DECKER SILSESQUIOXANE DERIVATIVE AND SYNTHESIZING METHOD THEREOF
-
Paragraph 0067-0069, (2020/10/10)
A double-deck silsesquioxane derivative ...
Blue light electroluminescent material and application thereof
-
, (2020/01/25)
The invention relates to a blue light el...
Preparation method and purification method of 9,10-substituted anthracene
-
, (2020/04/17)
The invention belongs to the technical f...
400607-04-7 Process route
-
-
7424-70-6
10-(naphthalen-1-yl)anthracene
-
-
400607-04-7
10-bromo-9-(naphthalene-1'-yl)anthracene
| Conditions | Yield |
|---|---|
|
With
N-Bromosuccinimide;
In
chloroform;
at 60 ℃;
for 3h;
Inert atmosphere;
|
98% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 2h;
|
97.5% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 2h;
|
97.5% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 2h;
|
92.2% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
|
92% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
|
92% |
|
With
N-Bromosuccinimide;
In
dichloromethane;
for 16h;
Inert atmosphere;
|
91% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 24h;
Inert atmosphere;
Reflux;
|
90% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 24h;
Reflux;
|
90% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
|
89% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 0.5h;
|
89% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide;
for 0.5h;
|
89% |
|
With
bromine;
In
dichloromethane;
|
88.3% |
|
With
N-Bromosuccinimide;
In
chloroform;
for 3h;
Reflux;
|
87% |
|
With
N-Bromosuccinimide;
In
1,2-dichloro-ethane;
at 0 - 10 ℃;
for 2h;
Inert atmosphere;
|
84.97% |
|
With
N-Bromosuccinimide;
In
N,N-dimethyl-formamide; chlorobenzene;
at 85 ℃;
for 3h;
|
82% |
|
With
bromine;
In
dichloromethane;
at 0 ℃;
|
76% |
|
With
bromine;
In
dichloromethane;
at 0 - 20 ℃;
|
76% |
|
With
bromine;
In
dichloromethane;
at 0 - 20 ℃;
|
76% |
|
With
bromine;
In
dichloromethane;
at 0 ℃;
|
75% |
-
-
523-27-3
9,10-Dibromoanthracene
-
-
13922-41-3
1-Naphthylboronic acid
-
-
400607-04-7
10-bromo-9-(naphthalene-1'-yl)anthracene
| Conditions | Yield |
|---|---|
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran; water;
at 80 ℃;
for 2h;
|
80% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
water; toluene;
at 60 ℃;
for 0.333333h;
Inert atmosphere;
|
76.89% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran;
at 50 - 90 ℃;
Inert atmosphere;
|
62.1% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
toluene;
for 24h;
Inert atmosphere;
Reflux;
|
62% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
water; toluene;
for 24h;
Inert atmosphere;
Reflux;
|
62% |
|
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
ethanol; toluene;
at 100 ℃;
for 12h;
Inert atmosphere;
|
42% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran; water;
at 80 ℃;
for 8h;
Inert atmosphere;
|
|
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran; water;
|
400607-04-7 Upstream products
-
523-27-3
9,10-Dibromoanthracene
-
13922-41-3
1-Naphthylboronic acid
-
1564-64-3
9-Bromoanthracene
-
7424-70-6
10-(naphthalen-1-yl)anthracene
400607-04-7 Downstream products
-
1149804-35-2
4,4,5,5-tetramethyl-2-(10-naphthalene-1-yl-anthracene-9-yl)-[1,3,2]dioxaborolane
-
400607-46-7
9-(naphthalen-1-yl)anthracen-10-yl-10-boronic acid
-
1225375-02-9
C37H23N
-
1261580-75-9
9-(9-phenylcarbazole-3-yl)-10-(naphthalene-1-yl)anthracene
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