1268244-56-9
- Product Name：9-(4-chloro-6-phenyl-1,3,5-triazin-2-yl)-9H-carbazole
- Molecular Formula：
- Purity：99%
- Molecular Weight：356.814
Product Details;
CasNo： 1268244-56-9
Reputable factory supply 9-(4-chloro-6-phenyl-1,3,5-triazin-2-yl)-9H-carbazole 1268244-56-9 in bulk at low price
- Molecular Formula:C21H13ClN4
- Molecular Weight:356.814
1268244-56-9 Relevant articles
Organic compound, organic light emitting diode and device including compound
-
Paragraph 0377-0381, (2021/05/29)
The present disclosure relates to an org...
ORGANIC COMPOUND, ORGANIC LIGHT EMITTING DIODE AND ORGANIC LIGHT EMITTING DEVICE INCLUDING THE COMPOUND
-
Paragraph 0294-0295, (2021/06/04)
The present disclosure relates to an org...
Compound for organic optoelectronic device, composition for organic optoelectronic device, organic optoelectronic device, and display device
-
Paragraph 0208-0211, (2021/04/26)
The present invention relates to a compo...
Compound and organic electroluminescent device
-
Paragraph 0036, (2021/01/29)
The invention discloses a compound and a...
1268244-56-9 Process route
-
-
1700-02-3
2,4-dichloro-6-phenyl-1,3,5-triazine
-
-
86-74-8,105184-46-1,97960-57-1
9H-carbazole
-
-
1268244-56-9
9-(4-chloro-6-phenyl-1 ,3,5-triazin-2-yl)-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 0 ℃;
for 12h;
Inert atmosphere;
|
95% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 0 ℃;
for 12h;
Inert atmosphere;
|
95% |
|
With
sodium hydride;
In
tetrahydrofuran;
at 0 - 25 ℃;
for 2h;
Inert atmosphere;
|
91% |
|
9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
|
80% |
|
9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
for 13h;
|
80% |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
at 110 ℃;
for 12h;
Inert atmosphere;
|
70% |
|
9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
Inert atmosphere;
|
63.4% |
|
9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 1h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide; mineral oil;
at 0 - 20 ℃;
Inert atmosphere;
|
63.4% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
|
62.5% |
|
9H-carbazole;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 ℃;
for 1h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
Inert atmosphere;
|
62.3% |
|
9H-carbazole;
With
n-butyllithium;
In
hexane;
at -78 ℃;
for 1h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
tetrahydrofuran; hexane;
at 20 ℃;
for 1h;
Inert atmosphere;
|
62.3% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
|
62.5% |
|
9H-carbazole;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 1h;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 13h;
|
60% |
|
2,4-dichloro-6-phenyl-1,3,5-triazine;
With
sodium hydride;
In
N,N-dimethyl-formamide;
at 0 ℃;
for 0.5h;
Inert atmosphere;
9H-carbazole;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 3h;
Inert atmosphere;
|
50% |
|
9H-carbazole;
With
sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 20 ℃;
for 1h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 60 ℃;
for 0.666667h;
|
43.6% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
|
42% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 200 ℃;
for 12h;
|
42% |
|
With
sodium t-butanolate;
In
tetrahydrofuran;
at 20 ℃;
for 12h;
|
42% |
|
9H-carbazole;
With
sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
Inert atmosphere;
2,4-dichloro-6-phenyl-1,3,5-triazine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
at 60 ℃;
for 0.5h;
Inert atmosphere;
|
8.1 g |
|
With
tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate;
In
toluene;
for 5h;
Reflux;
Inert atmosphere;
|
|
|
With
palladium;
|
-
-
24209-95-8
9-(4,6-dichloro-1,3,5-triazin-2-yl)-9H-carbazole
-
-
98-80-6
phenylboronic acid
-
-
1268244-56-9
9-(4-chloro-6-phenyl-1 ,3,5-triazin-2-yl)-9H-carbazole
| Conditions | Yield |
|---|---|
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; water; toluene;
for 12h;
Reflux;
|
72% |
|
With
tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
1,4-dioxane; water; toluene;
for 12h;
Reflux;
|
72% |
1268244-56-9 Upstream products
-
1700-02-3
2,4-dichloro-6-phenyl-1,3,5-triazine
-
86-74-8
9H-carbazole
-
100-58-3
phenylmagnesium bromide
-
24209-95-8
9-(4,6-dichloro-1,3,5-triazin-2-yl)-9H-carbazole
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